Part 1 Basic Knowledge in Organic Chemistry Laboratory
1．1 Rules in laboratory
1．2 Prevention and treatment of the common accidents in laboratory
1．3 Requirements of preparation， record and report of experiments
1．4 Common lab equipment and apparatus
1．5 Waste disposal
Part 2 Basic Experimental Techniques
2．1 Preparation of organic compounds
2．2 The determination of physical constants of organic compounds
2．3 Separation and purification technology of organic compounds
2．4 Spectral analysis technology of organic compounds
Part 3 Experiments for Preparation of Organic Compound
3．1 Preparation of cyclohexene
3．2 Preparation of anhydrous ethanol
3．3 Preparation of n-butyl bromide
3．4 Preparation of n-butyl ether
3．5 Preparation of acetophenone
3．6 Preparation of aspirin
3．7 Preparation of cinnanfic acid
3．8 Preparation of n-butyl acetate
3．9 Preparation of isoamyl acetate
3．10 Synthesis of glycerol monostearate
3．11 Preparation of skin care cosmetic
3．12 Preparation of detergent
Part 4 Extraction， Separation and Identification of
Organic Compounds
4．1 Distilling 95% ethanol and measuring the boiling point
4．2 Recrystallization of benzoic acid
4．3 Purification of benzaldehyde
4．4 Isolation of caffeine from tea leaves
4．5 The extraction of limonene from orange peels
4．6 Separation of A and B by thin-layer chromatography
4．7 Separation of spinach pigments by column chromatography
4．8 Preparation and resolution for optical isomers of tris（ethylenediamine）
cobalt salts
4．9 Identification of sugar
4．10 Identification of amino acids and proteins
Reference
Appendix： Experimental Graphs and Properties of
Organic Solvents
I ． Distilling 95% ethanol and measuring the boiling point
II． Recrystallization of benzoic acid
III． Isolation of caffeine from tea leaves and sublimation
IV． Synthesis， isolation and purification of n-butyl acetate
V． Physical constant
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